The Handbook Of Differential Scanning Calorimetry

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• Author : Joseph D Menczel,Janusz Grebowicz
• Publisher : Butterworth-Heinemann
• Release Date : 2023-03-01
• Total pages : 876
• ISBN : 9780128113486
• File Size : 44,6 Mb
• Total Download : 283
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Download Handbook of Differential Scanning Calorimetry in PDF, Epub, and Kindle

Differential scanning calorimetry (DSC) is the most important thermal analysis technique used today and the most common thermal analysis instrument found in chemical characterization laboratories. DSC has become an everyday tool in characterization laboratories, but many researchers using this technique have a limited understanding of the true breadth of its capabilities. Up to now, there has been no book that would describe the application of DSC in all the various areas of materials chemistry. The Handbook of Differential Scanning Calorimetry has been written to fill that void. This book is designed to summarize the knowledge of differential scanning calorimetry so that materials researchers and application chemists are given both a better understanding of techniques , as well as a review of the full scope of its capabilities. It also discusses how to properly interpret the DSC thermograms data obtained. Included in this work is the most up-to-date information written by some of the leaders in the field. It is written not only to help users get the most out of their equipment, After reading this book, people in all chemical and biological areas will have a broad overview of this measuring technique, and will be able to utilize this analytical technique more efficiently. Provides a detail description of the theory behind differential scanning while simultaneously providing a wider breadth of understanding of the actual DSC technique Includes a review of the basics of heat flux and power compensation DSC’s, as well as separate chapters on inorganic and organic materials Reviews the most common commercial DSC instruments on the market and their uses, including TA Instruments, Perkin-Elmer, Hitachi, Mettler Toledo, Netzsch, and Setaram

• Author : G.W.H. Höhne,W. Hemminger,H.-J. Flammersheim
• Publisher : Springer Science & Business Media
• Release Date : 2013-06-29
• Total pages : 223
• ISBN : 9783662033029
• File Size : 45,5 Mb
• Total Download : 661
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Download Differential Scanning Calorimetry in PDF, Epub, and Kindle

Differential Scanning Calorimetry (DSC) is a well established measuring method which is used on a large scale in different areas of research, development, and quality inspection and testing. Over a large temperature range, thermal effects can be quickly identified and the relevant temperature and the characteristic caloric values determined using substance quantities in the mg range. Measurement values obtained by DSC allow heat capacity, heat of transition, kinetic data, purity and glass transition to be determined. DSC curves serve to identify substances, to set up phase diagrams and to determine degrees of crystallinity. This book provides, for the first time, an overall description of the most impor tant applications of Differential Scanning Calorimetry. Prerequisites for reliable measurement results, optimum evaluation of the measurement curves and esti mation of the uncertainties of measurement are, however, the knowledge of the theoretical bases of DSC, a precise calibration of the calorimeter and the correct analysis of the measurement curve. The largest part of this book deals with these basic aspects: The theory of DSC is discussed for both heat flux and power compensated instruments; temperature calibration and caloric calibration are described on the basis of thermodynamic principles. Desmearing of the measurement curve in different ways is presented as a method for evaluating the curves of fast transitions.

• Author : Michael E. Brown
• Publisher : Elsevier
• Release Date : 1998-09-07
• Total pages : 722
• ISBN : 0080539599
• File Size : 36,9 Mb
• Total Download : 920
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Download Handbook of Thermal Analysis and Calorimetry in PDF, Epub, and Kindle

Handbook of Thermal Analysis and Calorimetry, Volume 1: Principles and Practice describes the basic background information common to thermal analysis and calorimetry in general. Thermodynamic and kinetic principles are discussed along with the instrumentation and methodology associated with thermoanalytical and calorimetric techniques. The purpose is to collect the discussion of these general principles and minimize redundancies in the subsequent volumes that are concerned with the applications of these principles and methods. More unique methods, which pertain to specific processes or materials, are covered in later volumes.

• Author : Anonim
• Publisher : Elsevier
• Release Date : 2018-03-12
• Total pages : 860
• ISBN : 9780444640635
• File Size : 10,6 Mb
• Total Download : 142
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Download Handbook of Thermal Analysis and Calorimetry in PDF, Epub, and Kindle

Handbook of Thermal Analysis and Calorimetry: Recent Advances, Techniques and Applications, Volume Six, Second Edition, presents the latest in a series that has been well received by the thermal analysis and calorimetry community. This volume covers recent advances in techniques and applications that complement the earlier volumes. There has been tremendous progress in the field in recent years, and this book puts together the most high-impact topics selected for their popularity by new editors Sergey Vyazovkin, Nobuyoshi Koga and Christoph Schick—all editors of Thermochimica Acta. Among the important new techniques covered are biomass conversion; sustainable polymers; polymer nanocompsoties; nonmetallic glasses; phase change materials; propellants and explosives; applications to pharmaceuticals; processes in ceramics, metals, and alloys; ionic liquids; fast-scanning calorimetry, and more. Features 19 all-new chapters to bring readers up to date on the current status of the field Provides a broad overview of recent progress in the most popular techniques and applications Includes chapters authored by a recognized leader in each field and compiled by a new team of editors, each with at least 20 years of experience in the field of thermal analysis and calorimetry Enables applications across a wide range of modern materials, including polymers, metals, alloys, ceramics, energetics and pharmaceutics Overviews the current status of the field and summarizes recent progress in the most popular techniques and applications

• Author : Anonim
• Publisher : Elsevier
• Release Date : 2011-09-22
• Total pages : 780
• ISBN : 0080556310
• File Size : 27,9 Mb
• Total Download : 454
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Download Handbook of Thermal Analysis and Calorimetry in PDF, Epub, and Kindle

This is Volume 5 of a Handbook that has been well-received by the thermal analysis and calorimetry community. All chapters in all five volumes are written by international experts in the subject. The fifth volume covers recent advances in techniques and applications that complement the earlier volumes. The chapters refer wherever possible to earlier volumes, but each is complete in itself. The latest recommendations on Nomenclature are also included. Amongst the important new techniques that are covered are micro-thermal analysis, pulsed thermal analysis, fast-scanning calorimetery and the use of quartz-crystal microbalances. There are detailed reviews of heating - stage spectroscopy, the range of electrical techniques available, applications in rheology, catalysis and the study of nanoparticles. The development and application of isoconversional methods of kinetic analysis are described and there are comprehensive chapters on the many facets of thermochemistry and of measuring thermophysical properties. Applications to inorganic and coordination chemistry are reviewed, as are the latest applications in medical and dental sciences, including the importance of polymorphism. The volume concludes with a review of the use and importance of thermal analysis and calorimetry in quality control. * Updates and complements previous volumes * Internationally recognized experts as authors * Each chapter complete in itself

• Author : M.E. Brown
• Publisher : Springer Science & Business Media
• Release Date : 2006-04-11
• Total pages : 264
• ISBN : 9780306484049
• File Size : 36,7 Mb
• Total Download : 699
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Download Introduction to Thermal Analysis in PDF, Epub, and Kindle

to Thermal Analysis Techniques and Applications Edited by Michael E. Brown Chemistry Department, Rhodes University, Grahamstown, South Africa KLUWER ACADEMIC PUBLISHERS NEW YORK, BOSTON, DORDRECHT, LONDON, MOSCOW eBook ISBN: 0-306-48404-8 Print ISBN: 1-4020-0472-9 ©2004 Kluwer Academic Publishers New York, Boston, Dordrecht, London, Moscow Print ©2001 Kluwer Academic Publishers Dordrecht All rights reserved No part of this eBook may be reproduced or transmitted in any form or by any means, electronic, mechanical, recording, or otherwise, without written consent from the Publisher Created in the United States of America Visit Kluwer Online at: http://kluweronline. com and Kluwer's eBookstore at: http://ebooks. kluweronline. com CONTENTS Preface to the First Edition, Chapman & Hall, London, 1988 ix About the First Edition of this Book x Preface to the Second Edition xi 1. INTRODUCTION 1. 1 Definition and History 1 1. 2 Thermal Analysis Instruments 4 References 11 2. THERMAL EVENTS 2. 1 Introduction 13 2. 2 The Solid State 13 2. 3 Reactions of Solids 14 2. 4 Decomposition of Solids 15 2. 5 Reaction with the Surrounding Atmosphere 16 2. 6 Solid-Solid Interactions 16 References 17 3. THERMOGRAVIMETRY (TG) Introduction 3. 1 19 3. 2 The Balance 19 3. 3 Heating the Sample 21 3. 4 The Atmosphere 24 3. 5 The Sample 26 3. 6 Temperature Measurement 26 3. 7 Temperature Control 28 Sample Controlled Thermal Analysis (SCTA) 29 3. 8 3. 9 Calibration 36 3. 10 Presentation of TG Data 37 3.

• Author : T. Hatakeyama,Liu Zhenhai
• Publisher : John Wiley & Sons
• Release Date : 1998
• Total pages : 480
• ISBN : UOM:39015046010750
• File Size : 30,6 Mb
• Total Download : 863
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Download Handbook of Thermal Analysis in PDF, Epub, and Kindle

Handbook of Thermal Analysis Edited by T. Hatakeyama National Institute of Materials and Chemical Research, Ibaraki, Japan Zhenhai Liu Changchun Institute of Applied Chemistry, China This 425-page reference book covers a comprehensive description of the principles of thermal analysis (TA) instruments, operating conditions, and the nature of the experimental data. Presented in a compact and well-arranged style with a large number of figures and illustrations, this work is divided into two parts. Part I is designed to acquaint and orient newcomers with TA by providing a comprehensive introduction to the basic principles of instrument operation, with advice on sample preparation and optimization of operating conditions, and a guide to interpreting results. The text deals primarily with techniques such as differential scanning calorimetry (DSC), differential thermal analysis (DTA), and thermogravimetry (TG). Part II illustrates 500 TA curves covering metals, inorganic and organic minerals, polymers, construction materials, pharmaceuticals, explosives, etc. The appendices include a glossary of TA terms, a survey of reference materials, the current table of TA standards, and a TA database. This book is aimed at advanced users and specialists who utilize TA methods for practical purposes, especially in research laboratories both academic and industrial. With an emphasis on practical instruction, industrial research staff, undergraduates and postgraduate students in the relevant fields will find this work a useful introduction to principle TA techniques.

• Author : V.S. Ramachandran,Ralph M. Paroli,James J. Beaudoin,Ana H. Delgado
• Publisher : William Andrew
• Release Date : 2002-10-28
• Total pages : 702
• ISBN : 9780815517757
• File Size : 44,7 Mb
• Total Download : 787
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Download Handbook of Thermal Analysis of Construction Materials in PDF, Epub, and Kindle

This comprehensive book containing essential information on the applicability of thermal analysis techniques to evaluate inorganic and organic materials in construction technology should serve as a useful reference for the scientist, engineer, construction technologist, architect, manufacturer, and user of construction materials, standard-writing bodies, and analytical chemists. The material scientists at the National Research Council of Canada have established one of the best thermal analysis laboratories in the world. Various types of thermal analysis techniques have been applied successfully to the investigation of inorganic and organic construction materials. These studies have provided important information on the characterization of raw as well as finished materials, quality control, quantitative estimation, interrelationships between physical, chemical, mechanical, and durability characteristics. Information on the application of thermal analysis to construction materials is dispersed in literature and hence the IRC scientists embarked on producing a handbook, the first of its kind, incorporating the latest knowledge available in this field of activity. Almost all important construction materials have been included.

• Author : Matthias Wagner
• Publisher : Unknown
• Release Date : 2017-12
• Total pages : 352
• ISBN : 1569906432
• File Size : 28,9 Mb
• Total Download : 630
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Download Thermal Analysis in Practice in PDF, Epub, and Kindle

Thermal analysis comprises a group of techniques used to determine the physical or chemical properties of a substance as it is heated, cooled, or held at constant temperature. It is particularly important for polymer characterization, but also has major application in analysis of pharmaceuticals and foodstuffs. This comprehensive handbook presents practical and theoretical aspects of the key techniques of DSC, TGA, TMA, DMA, and related methods. It also includes separate chapters on the glass transition, polymers, polymorphism, purity determination, and method development. The large number of practical examples included should inspire readers toward new ideas for applications in their own fields of work. The chapters are independent of one another and can be read individually in any desired order. Based on years of experience in thermal analysis of users, application specialists, consultants, and course instructors, this book provides practical help to newcomers, inexperienced users, and anyone else interested in the practical aspects of thermal analysis.

• Author : Joseph D. Menczel,R. Bruce Prime
• Publisher : John Wiley & Sons
• Release Date : 2014-07-09
• Total pages : 696
• ISBN : 9781118995990
• File Size : 34,5 Mb
• Total Download : 888
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Download Thermal Analysis of Polymers in PDF, Epub, and Kindle

Presents a solid introduction to thermal analysis, methods,instrumentation, calibration, and application along with thenecessary theoretical background. Useful to chemists, physicists, materials scientists, andengineers who are new to thermal analysis techniques, and toexisting users of thermal analysis who wish expand their experienceto new techniques and applications Topics covered include Differential Scanning Calorimetry andDifferential Thermal Analysis (DSC/DTA), Thermogravimetry,Thermomechanical Analysis and Dilatometry, Dynamic MechanicalAnalysis, Micro-Thermal Analysis, Hot Stage Microscopy, andInstrumentation. Written by experts in the various areas of thermalanalysis Relevant and detailed experiments and examples follow eachchapter.

• Author : Michael E. Brown,Patrick K. Gallagher
• Publisher : Elsevier Science
• Release Date : 2003-12-22
• Total pages : 942
• ISBN : 0444820868
• File Size : 35,8 Mb
• Total Download : 445
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Download Handbook of Thermal Analysis and Calorimetry in PDF, Epub, and Kindle

This is the second volume of a four volume set intended to describe the techniques and applications of thermoanalytical and calorimetric methods. The general techniques and methodology are covered extensively in Volume 1, along with the fundamental physicochemical background needed. Consequently the subsequent volumes dwell on the applications of these powerful and versatile methods, while assuming a familiarity with the techniques. Volume 2 covers major areas of inorganic materials and some related general topics, e.g., catalysis, geochemistry, and the preservation of art. The chapters are written by established practitioners in the field with the intent of presenting a sampling of the how thermoanalytical and calorimetric methods have contributed to progress in their respective areas. The chapters are not intended as exhaustive reviews of the topics, but rather, to illustrate to the readers what has been achieved and to encourage them to consider extending these applications further into their domains of interest. - Provides an appreciation for how thermal methods can be applied to inorganic materials and processes. - Provides an insight into the versatility of thermal methods. - Shares the experiences of experts in a variety of different fields. - A valuable reference source covering a huge area of materials coverage.

• Author : Michio Sorai
• Publisher : John Wiley & Sons
• Release Date : 2004-09-03
• Total pages : 570
• ISBN : UVA:X004805632
• File Size : 12,7 Mb
• Total Download : 444
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Download Comprehensive Handbook of Calorimetry and Thermal Analysis in PDF, Epub, and Kindle

Publisher Description

• Author : Steven M. Kurtz
• Publisher : Academic Press
• Release Date : 2009-04-27
• Total pages : 568
• ISBN : 008088444X
• File Size : 43,6 Mb
• Total Download : 655
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Download UHMWPE Biomaterials Handbook in PDF, Epub, and Kindle

UHMWPE Biomaterials Handbook describes the science, development, properties and application of of ultra-high molecular weight polyethylene (UHMWPE) used in artificial joints. This material is currently used in 1.4 million patients around the world every year for use in the hip, knee, upper extremities, and spine. Since the publication of the 1st edition there have been major advances in the development and clinical adoption of highly crosslinked UHMWPE for hip and knee replacement. There has also been a major international effort to introduce Vitamin E stabilized UHMWPE for patients. The accumulated knowledge on these two classes of materials are a key feature of the 2nd edition, along with an additional 19 additional chapters providing coverage of the key engineering aspects (biomechanical and materials science) and clinical/biological performance of UHMWPE, providing a more complete reference for industrial and academic materials specialists, and for surgeons and clinicians who require an understanding of the biomaterials properties of UHMWPE to work successfully on patient applications. The UHMWPE Handbook is the comprehensive reference for professionals, researchers, and clinicians working with biomaterials technologies for joint replacement New to this edition: 19 new chapters keep readers up to date with this fast moving topic, including a new section on UHMWPE biomaterials; highly crosslinked UHMWPE for hip and knee replacement; Vitamin E stabilized UHMWPE for patients; clinical performance, tribology an biologic interaction of UHMWPE State-of-the-art coverage of UHMWPE technology, orthopedic applications, biomaterial characterisation and engineering aspects from recognised leaders in the field

• Author : Richard B. Kemp
• Publisher : Elsevier
• Release Date : 1999-12-13
• Total pages : 1032
• ISBN : 0080535690
• File Size : 12,8 Mb
• Total Download : 802
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Download Handbook of Thermal Analysis and Calorimetry in PDF, Epub, and Kindle

The applications and interest in thermal analysis and calorimetry have grown enormously during the last half of the 20th century. These techniques have become indispensable in the study of processes such as catalysis, hazards evaluation etc., and in measuring important physical properties quickly, conveniently and with markedly improved accuracy. Consequently, thermal analysis and calorimetry have grown in stature and more scientists and engineers have become at least part-time, practitioners. People new to the field therefore need a source of information describing the basic principles and current state of the art. The last volume of this 4 volume handbook, devoted to many aspects of biological thermal analysis and calorimetry, completes a comprehensive review of this important area. All chapters have been prepared by recognized experts in their respective fields. The approach taken is "how and what to do and when to do it". The complete work is a valuable addition to the already existing literature.

• Author : Peter Haines
• Publisher : Royal Society of Chemistry
• Release Date : 2007-10-31
• Total pages : 234
• ISBN : 9781847551764
• File Size : 52,8 Mb
• Total Download : 145
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Download Principles of Thermal Analysis and Calorimetry in PDF, Epub, and Kindle

The use of thermal and calorimetric methods has shown rapid growth over the last two decades, in an increasingly wide range of applications. In addition, a number of powerful new techniques have been developed. This book supplies a concise and readable account of the principles, experimental apparatus and practical procedures used in thermal analysis and calorimetric methods of analysis. Brief accounts of the basic theory are reinforced with detailed applications of the methods and contemporary developments. Also included is information on standard test methods and manufacturers. Written by acknowledged experts, Principles of Thermal Analysis and Calorimetry is up-to-date, wide-ranging and practical. It will be an important source of information for many levels of readership in a variety of areas, from students and lecturers through to industrial and laboratory staff and consultants.

• Author : Imre Miklós Szilágyi,György Liptay
• Publisher : Springer
• Release Date : 2014-11-18
• Total pages : 363
• ISBN : 9783319094861
• File Size : 23,7 Mb
• Total Download : 776
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Download Who is Who in Thermal Analysis and Calorimetry in PDF, Epub, and Kindle

This is an expanded and revised second edition, presenting accurate and comprehensive information about our leading thermal scientists to current and future generations. In our globalized world, most researchers in thermal analysis do not know each other in person and are not familiar with each other’s achievements. This volume provides the reader with an up-to-date list of the prominent members in this community. The publication contains only living scientists. The selection is based partly on several decades of the editors' personal professional experience and also partly on the opinion of the Regional Editors of the Journal of Thermal Analysis and Calorimetry.

• Author : Christoph Schick,Vincent Mathot
• Publisher : Springer
• Release Date : 2016-06-28
• Total pages : 801
• ISBN : 9783319313290
• File Size : 21,6 Mb
• Total Download : 803
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Download Fast Scanning Calorimetry in PDF, Epub, and Kindle

In the past decades, the scan rate range of calorimeters has been extended tremendously at the high end, from approximately 10 up to 10 000 000 °C/s and more. The combination of various calorimeters and the newly-developed Fast Scanning Calorimeters (FSC) now span 11 orders of magnitude, by which many processes can be mimicked according to the time scale(s) of chemical and physical transitions occurring during cooling, heating and isothermal stays in case heat is exchanged. This not only opens new areas of research on polymers, metals, pharmaceuticals and all kinds of substances with respect to glass transition, crystallization and melting phenomena, it also enables in-depth study of metastability and reorganization of samples on an 1 to 1000 ng scale. In addition, FSC will become a crucial tool for understanding and optimization of processing methods at high speeds like injection molding. The book resembles the state-of-the art in Thermal Analysis & Calorimetry and is an excellent starting point for both experts and newcomers in the field.

• Author : Stephen Z.D. Cheng
• Publisher : Elsevier
• Release Date : 2002-12-09
• Total pages : 858
• ISBN : 008052740X
• File Size : 13,6 Mb
• Total Download : 951
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Download Handbook of Thermal Analysis and Calorimetry in PDF, Epub, and Kindle

As a new and exciting field of interdisciplinary macromolecular science and engineering, polymeric materials will have a profound presence in 21st century chemical, pharmaceutical, biomedical, manufacturing, infrastructure, electronic, optical and information technologies. The origin of this field derived from an area of polymer science and engineering encompassing plastic technologies. The field is rapidly expanding to incorporate new interdisciplinary research areas such as biomaterials, macromolecular biology, novel macromolecular structures, environmental macromolecular science and engineering, innovative and nano-fabrications of products, and is translating discoveries into technologies. · Unique in combining scientific concepts with technological aspects · Provides a comprehensive and broad coverage of thermodynamic and thermal behaviours of various polymeric materials as well as methodologies of thermal analysis and calorimetry · Contributions are from both pioneering scientists and the new generation of researchers

• Author : Emma Chiavaro
• Publisher : CRC Press
• Release Date : 2014-12-02
• Total pages : 301
• ISBN : 9781466591530
• File Size : 24,8 Mb
• Total Download : 553
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Download Differential Scanning Calorimetry in PDF, Epub, and Kindle

Differential Scanning Calorimetry: Applications in Fat and Oil Technology provides a complete summary of the scientific literature about differential scanning calorimetry (DSC), a well-known thermo-analytical technique that currently has a large set of applications covering several aspects of lipid technology. The book is divided into three major sections. The first section covers the applications of DSC to study cooling and heating profiles of the main source of oils and fats. The second is more theoretical, discussing the application of DSC coupled to related thermal techniques and other physical measurements. And the third covers specific applications of DSC in the field of quality evaluation of palm, palm kernel, and coconut oils and their fractions as well as of some other important aspects of lipid technology such as shortening and margarine functionality, chocolate technology, and food emulsion stability. This book is a helpful resource for academicians, food scientists, food engineers and technologists, food industry operators, government researchers, and regulatory agencies.

• Author : Mike Reading,Douglas J. Hourston
• Publisher : Springer Science & Business Media
• Release Date : 2006-10-12
• Total pages : 330
• ISBN : 9781402037504
• File Size : 15,7 Mb
• Total Download : 681
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Download Modulated Temperature Differential Scanning Calorimetry in PDF, Epub, and Kindle

MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of the sample’s heat capacity from the modulation. The new information this provided sparked a revolution in scanning calorimetry by enabling new insights to be gained into almost all aspects of polymer characteristics. This book provides both a basic and advanced treatment of the theory of the technique followed by a detailed exposition of its application to reacting systems, blends and semicrystalline polymers by the leaders in all of these fields. It is an essential text for anybody interested in calorimetry or polymer characterization, especially if they have found that conventional DSC cannot help them with their problems.

• Author : Simon Gaisford,Vicky Kett,Peter Haines
• Publisher : Royal Society of Chemistry
• Release Date : 2016-02-25
• Total pages : 280
• ISBN : 9781782620518
• File Size : 46,5 Mb
• Total Download : 288
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Download Principles of Thermal Analysis and Calorimetry in PDF, Epub, and Kindle

This book supplies an up to date, concise and readable account of the principles, experimental apparatus and practical procedures used in thermal analysis and calorimetric methods of analysis and will be an aid for students and lecturers through to industrial and laboratory staff and consultants.