Forced Flow Layer Chromatography

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• Author : Erno Tyihak
• Publisher : Elsevier
• Release Date : 2015-12-01
• Total pages : 524
• ISBN : 9780124202122
• File Size : 38,7 Mb
• Total Download : 822
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Download Forced-Flow Layer Chromatography in PDF, Epub, and Kindle

Forced-Flow Layer Chromatography takes a close look at the specifics of forced-flow layer chromatography techniques, from their evolution to the nuances of using these techniques in a variety of applications where traditional thin-layer chromatography (TLC) and high-performance thin-layer chromatography (HPTLC) are not as effective. This book presents a number of variations of TLC techniques, with special emphasis on the overpressured-layer chromatography (OPLC) technique and newer developments such as the BioArena System for biomedical analysis. The versatility of these forced-flow techniques opens up new avenues for the analysis of a large number of samples for high-throughput screening and for the analysis of very complex matrices, while the development of BioArena extends the use of these techniques to challenging new areas of bioanalysis. Details a variety of forced-flow techniques, explaining how they markedly reduce developing time and result in less lateral diffusion and more compact spots Emphasizes the benefits of OPLC separation techniques, a method pioneered by the authors nearly forty years ago Discusses new developments, such as the BioArena system used to facilitate detection, isolation, and identification of new antimicrobials, antineoplastics, biopesticides, and other biologically active substances

• Author : Colin Poole
• Publisher : Elsevier
• Release Date : 2014-09-22
• Total pages : 652
• ISBN : 9780124172845
• File Size : 37,9 Mb
• Total Download : 933
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Download Instrumental Thin-Layer Chromatography in PDF, Epub, and Kindle

Instrumental Thin-Layer Chromatography delivers comprehensive coverage of this separation tool with particular emphasis on how this tool can be used in advanced laboratories and integrated into problem-solving scenarios. Significant improvements in instrumentation have outpaced the development of information resources that describe the latest state-of-the-art and demonstrate the full capabilities of TLC. This book provides a contemporary picture of the fundamentals and practical applications of TLC at a level suitable for the needs of professional scientists with interests in project management where TLC is a common tool. Compact, highly focused chapters convey essential information that defines modern TLC and how it can be effectively implemented in most areas of laboratory science. Numerous figures and tables provide access to material not normally found in a single source yet are required by working scientists. Contributions written by recognized authoritative and visionary experts Focuses on state-of-the-art instrumental thin-layer chromatography and advanced applications across many areas Provides guidance on the analysis of complex, dirty mixtures of compounds Offers a cost-effective analytic technique for laboratories working under strict budgets

• Author : Monika Waksmundzka-Hajnos,Joseph Sherma,Teresa Kowalska
• Publisher : CRC Press
• Release Date : 2008-03-04
• Total pages : 896
• ISBN : 1420046780
• File Size : 12,8 Mb
• Total Download : 278
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Download Thin Layer Chromatography in Phytochemistry in PDF, Epub, and Kindle

Thin layer chromatography (TLC) is increasingly used in the fields of plant chemistry, biochemistry, and molecular biology. Advantages such as speed, versatility, and low cost make it one of the leading techniques used for locating and analyzing bioactive components in plants. Thin Layer Chromatography in Phytochemistry is the first source devoted to supplying state-of-the-art information on TLC as it applies to the separation, identification, quantification, and isolation of medicinal plant components. Renowned scientists working with laboratories around the world demonstrate the applicability of TLC to a remarkable diversity of fields including plant genetics, drug discovery, nutraceuticals, and toxicology. Elucidates the role of plant materials in the pharmaceutical industry... Part I provides a practical review of techniques, relevant materials, and the particular demands for using TLC in phytochemical applications. The text explains how to determine the biological activity of metabolites and assess the effectiveness of herbal medicines and nutritional supplements. Part II concentrates on TLC methods used to analyze specific plant-based metabolite classes such as carbohydrates, proteins, alkaloids, flavonoids, terpenes, etc. Organized by compound type, each chapter discusses key topics such as sample preparation, plate development, zone detection, densitometry, and biodetection. Demonstrates practical methods that can be applied to a wide range of disciplines... From identification to commercial scale production and quality control, Thin Layer Chromatography in Phytochemistry is an essential bench-top companion and reference on using TLC for the study of plant-based bioactive compounds.

• Author : Colin Poole
• Publisher : Elsevier
• Release Date : 2023-01-01
• Total pages : 692
• ISBN : 9780323983013
• File Size : 44,7 Mb
• Total Download : 334
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Download Instrumental Thin-Layer Chromatography in PDF, Epub, and Kindle

Instrumental Thin-Layer Chromatography, Second Edition offers a comprehensive source of authoritative information on all aspects of instrumental thin-layer chromatography. The use of short, topic-focused chapters facilitates identifying information of immediate interest for familiar or emerging uses of thin-layer chromatography. The book gives those working in both academia and industry the opportunity to learn, refresh, or deepen their understanding of fundamental and instrumental aspects of thin-layer chromatography, as well as the tools to interpret and manage chromatographic data. The book serves as a practical consolidated guide to the selection of separation conditions and the use of auxiliary techniques. This fully updated new edition restores the contemporary character of the book for those involved in advancing the technology, analyzing data produced, or applying the technique to new application areas. Some chapters have been consolidated to make room for topics not covered in the first edition, reflecting general changes in the field of thin-layer chromatography, especially in effects-directed detection, convenient interfaces for advanced spectroscopic detection, and greater automation possibilities. This book is a valuable reference for anyone who needs to acquire fundamental and practical information to facilitate progress in research and management functions utilizing information acquired by thin-layer chromatography. Features individual chapters written by recognized authoritative and visionary experts in the field Provides an overview and focused treatment of a single topic Provides tables and diagrams with commonly used data to facilitate practical work, comparison of results, and decision-making Places modern developments in the research literature into a general context not always apparent to inexperienced users of the technique Offers comprehensive updates to all chapters Includes new chapters on instrument platforms, effects-directed detection, data analysis tools, small-scale and microfluidic planar separation systems, and applications to the separation of amino acids and peptides, the analysis of saccharides and lipids, and forensic analysis

• Author : Robert J. Flanagan,Andrew A. Taylor,Ian D. Watson,Robin Whelpton
• Publisher : John Wiley & Sons
• Release Date : 2008-03-03
• Total pages : 605
• ISBN : 9780470319345
• File Size : 35,7 Mb
• Total Download : 541
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Download Fundamentals of Analytical Toxicology in PDF, Epub, and Kindle

The analytical toxicologist may be required to detect, identify, and in many cases measure a wide variety of compounds in samples from almost any part of the body or in related materials such as residues in syringes or in soil. This book gives principles and practical information on the analysis of drugs and poisons in biological specimens, particularly clinical and forensic specimens. After providing some background information the book covers aspects of sample collection, transport, storage and disposal, and sample preparation. Analytical techniques - colour tests and spectrophotometry, chromatography and electro­phoresis, mass spectrometry, and immunoassay – are covered in depth, and a chapter is devoted to the analysis of trace elements and toxic metals. General aspects of method implementation/validation and laboratory operation are detailed, as is the role of the toxicology laboratory in validating and monitoring the performance of point of care testing (POCT) devices. The book concludes with reviews of xenobiotic absorption, distribution and metabolism, pharmacokinetics, and general aspects of the interpretation of analytical toxicology results. A clearly written, practical, integrated approach to the basics of analytical toxicology. Focuses on analytical, statistical and pharmacokinetic principles rather than detailed applications. Assumes only a basic knowledge of analytical chemistry. An accompanying website provides additional material and links to related sites. Written by an experienced team of authors,Fundamentals of Analytical Toxicology is an invaluable resource for those starting out in a career in analytical toxicology across a wide range of disciplines including clinical and forensic science, food safety, and pharmaceutical development. Praise from the reviews: “This is an ambitious effort to describe in detail the many and varied aspects of the science of toxicological analysis. The 17 chapters cover every foreseeable aspect, from specimen collection through analytical techniques and quality control to pharmacological principles and interpretation of results. The authors bring together a great deal of experience in the field and have succeeded admirably in achieving their goal: "to give principles and practical information on the analysis of drugs, poisons and other relevant analytes in biological specimens...". The book is very readable and quite up-to-date, and contains many illustrative figures, charts and tables. Both the student and the practicing professional would do well to study this material carefully, as there is something here for every conceivable level of interest.” Review from Randall Baselt "This text comes highly recommended for any analytical toxicology trainee." The Bulletin of the Royal College of Pathologists “Overall, this book provides a comprehensive, thorough, clear, up to date and practical treatment of analytical toxicology at a high standard. Understanding of the text is enhanced by the use of many illustrations. Specifications, guidelines, and methods are highlighted in grey background “Boxes”. The many and up to date literature references in each chapter demonstrate the authors’ thorough work and permit easy access to deeper information. Therefore this book can be highly recommended as a valuable source of knowledge in analytical toxicology both as an introduction and for the advanced reader.” GTFCh Bulletin “Toxichem + Krimtech”, May 2008 (translated, original review in German) “Many toxicologists will add this important reference to their libraries because it competently fills a need ...” International Journal of Toxicology “The book is very well illustrated, easy to understand and pleasant to read, and contains a wealth of dedicated information.” International Journal of Environmental Analytical Chemistry

• Author : Joseph Sherma,Bernard Fried
• Publisher : CRC Press
• Release Date : 2003-04-18
• Total pages : 1356
• ISBN : 9780824748661
• File Size : 53,8 Mb
• Total Download : 761
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Download Handbook of Thin-Layer Chromatography in PDF, Epub, and Kindle

In this third edition, more than 40 renowned authorities introduce and update chapters on the theory, fundamentals, techniques, and instrumentation of thin-layer chromatography (TLC) and high-performance thin-layer chromatography (HPTLC), highlighting the latest procedures and applications of TLC to 19 important compound classes and coverage of TLC applications by compound type. Easily adaptable to industrial scenarios , the Handbook of Thin-Layer Chromatography, Third Edition supports practical research strategies with extensive tables of data, offers numerous figures that illustrate techniques and chromatograms, and includes a glossary as well as a directory of equipment suppliers.

• Author : Peter E Wall
• Publisher : Royal Society of Chemistry
• Release Date : 2007-10-31
• Total pages : 204
• ISBN : 9781847552464
• File Size : 33,5 Mb
• Total Download : 600
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Download Thin-Layer Chromatography in PDF, Epub, and Kindle

Thin-Layer Chromatography (TLC) is a modern, reliable tool that complements other chromatographic techniques. This book provides a practical guide to the basic principles, procedures and pitfalls on the practical application of TLC. Thin Layer Chromatography: A Modern Practical Approach offers a sequence of chapters following the steps of the technique as the chromatographer would follow them. The chapters provide a choice of sorbent best suited to the separation intended, followed by pre-treatment required for the sample, applying the sample to the sorbent layer, development procedure, visualisation and detection, and finally quantification. Imaging and hyphenation techniques are described. The reasons why recommendations are made for specific and more general methods are covered. The book also provides an overview of some recent developments in the field.

• Author : Teresa Kowalska,Mieczyslaw Sajewicz,Joseph Sherma
• Publisher : CRC Press
• Release Date : 2015-11-18
• Total pages : 380
• ISBN : 9781498705899
• File Size : 32,7 Mb
• Total Download : 143
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Download Planar Chromatography - Mass Spectrometry in PDF, Epub, and Kindle

Planar Chromatography–Mass Spectrometry focuses on a relatively new approach to chemical analysis in general, and to separation science in particular. It is the first book to systemically cover the theoretical background, techniques, instrumentation, and practical applications of planar chromatography–mass spectrometry as a hyphenated tool of analytical chemistry. It also examines the high and as-yet unexploited potential of planar chromatography–mass spectrometry for analytical use in scientific investigations. This book overviews the combination of planar chromatography, a relatively simple and cost-effective separation step for determining complex mixtures of compounds, with mass spectrometry, an efficient, highly instrumental, and relatively expensive technique that enables rapid identification of separated chemical species. It covers electrophoretic–mass spectrometry methods and applications, which are considered planar chromatographic techniques and are increasingly being exploited in proteomic and molecular biology studies as well as for medical diagnostic purposes. It also provides a selection of applications, such as drug control and forensic and food analysis, including more difficult substances such as carbohydrates and lipids. The book advocates growth in using planar chromatography–mass spectrometry in laboratories that have appropriate equipment but have not yet employed the techniques in combination. It also describes the use of a relatively inexpensive commercial system that can be adopted by laboratories currently working without the coupled methodology. Aiming to improve power and efficiency when other analytical methods are inadequate, Planar Chromatography–Mass Spectrometry encourages separation science practitioners in academia and industry to combine the two methods for enhanced results.

• Author : Bernard Fried,Joseph Sherma
• Publisher : CRC Press
• Release Date : 1999-01-04
• Total pages : 475
• ISBN : 9780824742089
• File Size : 49,6 Mb
• Total Download : 798
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Download Thin-Layer Chromatography, Revised And Expanded in PDF, Epub, and Kindle

The fourth edition of this work emphasizes the general practices and instrumentation involving TLC and HPTLC, as well as their applications based on compound types, while providing an understanding of the underlying theory necessary for optimizing these techniques. The book details up-to-date qualitative and quantitative densitometric experiments on organic dyes, lipids, antibiotics, pharmaceuticals, organic acids, insecticides, and more.

• Author : Thomas Beesley,Benjamin Buglio
• Publisher : CRC Press
• Release Date : 2000-12-06
• Total pages : 322
• ISBN : 9780824745332
• File Size : 54,5 Mb
• Total Download : 978
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Download Quantitative Chromatographic Analysis in PDF, Epub, and Kindle

Highlights critical factors involved in successful chromatographic analysis. Details analytical procedures; outlining sample preparation, collection, transportation, and storage. Provides step-by-step guidelines for producing analytical reports.

• Author : Nelu Grinberg
• Publisher : CRC Press
• Release Date : 1990-04-27
• Total pages : 520
• ISBN : 0824781384
• File Size : 43,6 Mb
• Total Download : 506
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Download Modern Thin-Layer Chromatography in PDF, Epub, and Kindle

Provides chemists with an in-depth account of chromatographic phenomena and a detailed reference guide to the various choices in optimizing chromatographic separations of enantiomers. Clarifies how thin-layer chromatography differs from, but can be used as a pilot procedure for, high-performance liq

• Author : Teresa Kowalska,Joseph Sherma
• Publisher : CRC Press
• Release Date : 2006-02-03
• Total pages : 424
• ISBN : 9781420005820
• File Size : 46,9 Mb
• Total Download : 229
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Download Preparative Layer Chromatography in PDF, Epub, and Kindle

Preparative Layer Chromatography explains how this method is used for separating large quantities of mixtures containing a wide variety of important compounds. It offers a broad review of preparative layer chromatography (PLC) applications and adaptable working procedures for microseparations involving organic, inorganic, and organometallic compounds. The book contains theoretical background, chemical principles, and relevance of preparative layer chromatography (PLC) to a wide range of applications, particularly in the study of pharmaceuticals and biochemistry. Written by many of the best known and most knowledgeable specialists in the field, the chapters describe all the necessary techniques, current procedures, and superior strategies for selecting the most suitable eluents and designing application-specific PLC systems based on the data being sought. They provide comprehensive instructions, surrounding issues, and suggestions for optimizing optional working techniques within the framework of PLC. The book also provides a complete coverage of bulk sorbents and precoated chromatographic plates available on the international market. A comprehensive, yet accessible source of information, Preparative Layer Chromatography is a relevant and practical text for experienced as well as novice researchers and practitioners involved in analytical, environmental, geochemical, biological, medicinal, and pharmaceutical analysis.

• Author : Szabolcs Nyiredy
• Publisher : Unknown
• Release Date : 2001
• Total pages : 614
• ISBN : 963699157X
• File Size : 9,6 Mb
• Total Download : 746
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Download Planar Chromatography in PDF, Epub, and Kindle

PDF book entitled Planar Chromatography written by Szabolcs Nyiredy and published by Unknown which was released on 2001 with total hardcover pages 614, the book become popular and critical acclaim.

• Author : Kevin Robards,Danielle Ryan
• Publisher : Academic Press
• Release Date : 2021-05-01
• Total pages : 530
• ISBN : 9780128220979
• File Size : 29,7 Mb
• Total Download : 598
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Download Principles and Practice of Modern Chromatographic Methods in PDF, Epub, and Kindle

Principles and Practice of Modern Chromatographic Methods, Second Edition takes a comprehensive, unified approach in its presentation of chromatographic techniques. Like the first edition, the book provides a scientifically rigid, but easy-to-follow presentation of chromatography concepts that begins with the purpose and intent of chromatographic theory - the “what and why that are left out of other books attempting to cover these principles. This fully revised second edition brings the content up-to-date, covering recent developments in several new sections and an additional chapter on composite methods. New topics include sample profiling, sample preparation, sustainable green chemistry, 2D chromatography, miniaturization/nano-LC, HILIC, and more. Contains thorough chapters that begin with an updated schematic overview and a visual representation of the content Avoids the obfuscation of different terminologies and classification systems that are prevalent in the area, such as the relationship between liquid chromatography and column chromatography Provides integrated and comprehensive topic coverage based on chromatographic bibliometrics and survey reports on the relative usage of chromatographic techniques

• Author : Anonim
• Publisher : Academic Press
• Release Date : 2009-11-11
• Total pages : 880
• ISBN : 0123757274
• File Size : 34,7 Mb
• Total Download : 508
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Download Handbook of Methods and Instrumentation in Separation Science in PDF, Epub, and Kindle

Handbook of Methods and Instrumentation in Separation Science, Volume 1 provides concise overviews and summaries of the main methods used for separation. It is based on the Encyclopedia of Separation Science. The handbook focuses on the principles of methods and instrumentation. It provides general concepts concerning the subject matter; it does not present specific procedures. This volume discusses the separation processes including affinity methods, analytical ultracentrifugation, centrifugation, chromatography, and use of decanter centrifuge and dye. Each methodology is defined and compared with other separation processes. It also provides specific techniques, principles, and theories concerning each process. Furthermore, the handbook presents the applications, benefits, and validation of the processes described in this book. This handbook is an excellent reference for biomedical researchers, environmental and production chemists, flavor and fragrance technologists, food and beverage technologists, academic and industrial librarians, and nuclear researchers. Students and novices will also find this handbook useful for practice and learning. One-stop source for information on separation methods General overviews for quick orientation Ease of use for finding results fast Expert coverage of major separation methods Coverage of techniques for all sizes of samples, pico-level to kilo-level

• Author : E. Heftmann
• Publisher : Elsevier
• Release Date : 2004-04-16
• Total pages : 584
• ISBN : 9780080472249
• File Size : 41,9 Mb
• Total Download : 838
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Download Chromatography in PDF, Epub, and Kindle

Chromatography has emerged as the most important and versatile analytical method. The book is not only an updated version of Heftmann's classical text, but it covers areas of future importance, such as microfluidics and computer resources. Under his experienced guidance, authorities in each field have contributed their practical experience to an integrated treatment of modern micro analysis. In Part A the theoretical basis of individual separation methods is explained and the technical aspects are illustrated. It includes the theory of gas and liquid chromatography as well as specific chromatographic techniques, such as size-exclusion, planar, ion, and affinity chromatography as well as various electrokinetic separation techniques. Microfluidics are covered for the first time and useful sources of analytical instruments are listed and evaluated. 1. Each chapter written by an authority 2. Thorough treatment of the theoretical basis of separation methods 3. Practical guide for performing analyses

• Author : C. F. Poole
• Publisher : Elsevier
• Release Date : 2003
• Total pages : 952
• ISBN : 0444501991
• File Size : 40,6 Mb
• Total Download : 794
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Download The Essence of Chromatography in PDF, Epub, and Kindle

The Essence of Chromatography presents a comprehensive survey of modern chromatography and is intended as a suitable text for graduate level courses in the separation sciences and as a self-study guide for professional chromatographers wishing to refresh their background in this rapidly expanding field.This title is an effective replacement for Chromatography Today, written by the same author with Salwa K. Poole, which is considered to be one of the definitive chromatographic texts of the last decade. Its format is modular, with extensive cross-references to permit rapid location of re.

• Author : F.A.A. Dallas,H. Read,R.J. Ruane,I.D. Wilson
• Publisher : Springer Science & Business Media
• Release Date : 2013-11-09
• Total pages : 247
• ISBN : 9781489922212
• File Size : 26,6 Mb
• Total Download : 365
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Download Recent Advances in Thin-Layer Chromatography in PDF, Epub, and Kindle

For many years TLC has suffered from the image of being a low sensitivity, low resolution, non-quantitative teehnique, suitable for chemists, but not a tool for real ehromatographers. Whilst perhaps true in the past this attitude no longer ref1eets the eapabi1ities of modern instrumenta1ized TLC in all its many forms. This volume represents the proceedings of a meeting in Brighton in 1987 whieh formed part of a eontinuing series of one and two day events on TLC organized by the Chromatographie Soeiety either alone or, like this one, in eonjunetion with other learned bodies. These meetings are designed to keep ehromatographers up to date with the latest deve10pments and help promote a more positive image of TLC. lan Wilson November 1987 v CONTENTS The Chromatographic Society xi Contemporary Thin-layer Chromatography: An introduction IoD. Wilson INSTRUMENTATION Quantitative Methods in Thin-layer Chromatography C.F. Poole, S.K. Poole and T.A. Dean 11 Fluorescence Line-narrowing Spectroscopy: A New and Highly Selective Detection Technique for Thin-layer and Liquid Chromatography J.W. Hofstraat, C. Gooijer, U.A. Th. Brinkman and N.H. Velthorst 29 Qualitative and Quantitative Image Analysis of Fluorescence from High Performance Thi. n-layer Chromatography R.M. Belchamber, S.J. Brinkworth, H. Read and J.D.M. Roberts 37 Analytical Rotation Planar Chromatography Sz. Nyiredy, K. Dallenbach-Toelke and O. Sticher 45 Analytical and Preparative Overpressured Layer Chromatography E. Mincsovics and E. Tyihak 57 Anticircular Planar Chromatography: Analytical and Preparative Aspects H. Traitler and A.

• Author : Bernd Spangenberg,Colin F. Poole,Christel Weins
• Publisher : Springer Science & Business Media
• Release Date : 2011-01-03
• Total pages : 388
• ISBN : 9783642107290
• File Size : 9,7 Mb
• Total Download : 618
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Download Quantitative Thin-Layer Chromatography in PDF, Epub, and Kindle

Thin-layer chromatography (TLC) is widely used particularly for pharmaceutical and food analysis. While there are a number of books on the qualitative identification of chemical substances by TLC, the unique focus here is on quantitative analysis. The authors describe all steps of the analytical procedure, beginning with the basics and equipment for quantitative TLC followed by sample pretreatment and sample application, development and staining, scanning, and finally statistical and chemometric data evaluation and validation. An important feature is the coverage of effect-directed biological detection methods. Chapters are organized in a modular fashion facilitating the easy location of information about individual procedural steps.

• Author : Lukasz Komsta,Monika Waksmundzka-Hajnos,Joseph Sherma
• Publisher : CRC Press
• Release Date : 2013-12-20
• Total pages : 1067
• ISBN : 9781466507166
• File Size : 25,7 Mb
• Total Download : 876
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Download Thin Layer Chromatography in Drug Analysis in PDF, Epub, and Kindle

Used routinely in drug control laboratories, forensic laboratories, and as a research tool, thin layer chromatography (TLC) plays an important role in pharmaceutical drug analyses. It requires less complicated or expensive equipment than other techniques, and has the ability to be performed under field conditions. Filling the need for an up-to-date

• Author : Steven M. Colegate,Russell J. Molyneux
• Publisher : CRC Press
• Release Date : 2007-12-14
• Total pages : 624
• ISBN : 9781420006889
• File Size : 44,7 Mb
• Total Download : 597
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Download Bioactive Natural Products in PDF, Epub, and Kindle

Bioactive natural products are proving to be a rich source of novel therapeutics to both protect against and combat diseases, as well as serve as lead compounds in crop protection. Following the successful format of the first edition, this volume brings together collective research from many new contributors and emphasizes the rationale behind the